3-甲氧基-2-环己烯-1-酮合成路线 (共 49 条)
参考文献
Chemische Berichte, , vol. 85, p. 61,71
参考文献
Tetrahedron, , vol. 37, p. 1921 - 1926
参考文献
Tetrahedron, , vol. 37, p. 1921 - 1926
参考文献
Canadian Journal of Chemistry, , vol. 51, p. 843 - 847
反应条件
ammonium cerium(IV) nitrate in water; acetonitrile 0.5 h; Heating;
参考文献
Banerjee, Biplab; Mandal, Samir Kumar; Roy, Subhas Chandra
Chemistry Letters, 2006 , vol. 35, # 1 p. 16 - 17
反应条件
lithium aluminium tetrahydride; diethyl ether; water anschl. mit wss. H2SO4;
参考文献
Bl. Res. Coun. Israel, , vol. 2, p. 273
Journal of the Chemical Society, , p. 1779,1781
反应条件
chloro-trimethyl-silane; potassium hydride 1.) tetrahydrofuran, room t., 15 h, 0 degC, 15 min; 2.) from -78 to 50 degC over 1 h, 50 degC, 1 h; Yield given. Multistep reaction;
参考文献
Mcmurry,J.E.; Erion,M.D.
Journal of the American Chemical Society, 1985 , vol. 107, p. 2712
反应条件
1: With titanium(IV) isopropylate in diethyl ether T=20°C; 2: With water; ammonium chloride in diethyl ether 3: With toluene-4-sulfonic acid in diethyl ether T=20°C;
参考文献
Bamberg, Joe Timothy; Hermann, Johannes Cornellius; Lemoine, Remy; Soth, Michael
Patent: US2010/144745 A1, 2010 ;
Location in patent: Page/Page column 43 ;
US 20100144745 A1
反应条件
1: With titanium(IV) isopropylate in diethyl ether T=25°C; Kulinkivich cyclopropanation; 2: With toluene-4-sulfonic acid in diethyl ether; water
参考文献
Masalov, Nikolai; Feng, Wei; Jin, Kun Cha
Organic Letters, 2004 , vol. 6, # 14 p. 2365 - 2368
反应条件
1: 84 percent / LDA / tetrahydrofuran 2: DIBAL / hexane; CH2Cl2 / 2 h / Ambient temperature 3: H2 / 5percent Pd/C / propan-2-ol; methanol / 2 h View Scheme
参考文献
Smith, Amos B.; Nolen, Ernest G.; Shirai, Ryuichi; Blase, Frances R.; Ohta, Mitsuaki; et al.
Journal of Organic Chemistry, 1995 , vol. 60, # 24 p. 7837 - 7848