3-甲氧基-2-环己烯-1-酮合成路线 （共 49 条）
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane
T=0 - 20°C; 120 h;
参考文献
Kurdyumov, Aleksey V.; Lin, Nan; Hsung, Richard P.; Gullickson, Glen C.; Cole, Kevin P.; Sydorenko, Nadiya; Swidorski, Jacob J.
Organic Letters, 2006 , vol. 8, # 2 p. 191 - 193
反应条件
(i) Na, benzene, (ii) AcOH, (iii) aq. H2SO4; Multistep reaction;
参考文献
Bryson,T.A.; Wilson,C.A.
Synthetic Communications, 1976 , vol. 6, p. 521 - 526
参考文献
Bryson,T.A.; Wilson,C.A.
Synthetic Communications, 1976 , vol. 6, p. 521 - 526
反应条件
2: TsOH / benzene / Heating
View Scheme
参考文献
Bryson,T.A.; Wilson,C.A.
Synthetic Communications, 1976 , vol. 6, p. 521 - 526
反应条件
1: 84 percent / tetrahydrofuran; diethyl ether / 4 h / Ambient temperature
2: 59 percent / dimethylsulfoxide; tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Piers, Edward; Banville, Jacques; Lau, Cheuk Kun; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 2965 - 2975
反应条件
in tetrahydrofuran; diethyl ether
4 h; Ambient temperature;
参考文献
Piers, Edward; Banville, Jacques; Lau, Cheuk Kun; Nagakura, Isao
Canadian Journal of Chemistry, 1982 , vol. 60, p. 2965 - 2975
反应条件
in tetrahydrofuran; hexane
T=0°C; 12 h;
参考文献
Moritani, Yasunori; Appella, Daniel H.; Jurkauskas, Valdas; Buchwald, Stephen L.
Journal of the American Chemical Society, 2000 , vol. 122, # 28 p. 6797 - 6798
反应条件
n-butyllithium in hexane
参考文献
Massachusetts Institute of Technology
Patent: US6465664 B1, 2002 ;
反应条件
diethyl ether; benzene
参考文献
Nasarow; Saw'jalow
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1958 , p. 1233,1236;engl.Ausg.S.1190,1193
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1957 , p. 207,211;engl.Ausg.S.219,222
