2-(1-金刚烷)-1H-异吲哚-1,3(2H)-二酮合成路线 (共 11 条)
反应条件
triethylamine; 3-diphenyloxyphosphinyl-2-oxazolidinone in acetonitrile
T=40°C; 0.5 h;
参考文献
Abdel-Aziz, Alaa A.-M.
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 5 p. 614 - 626
反应条件
triethylamine; 3-diphenyloxyphosphinyl-2-oxazolidinone in acetonitrile
T=40°C; 0.333333 h;
参考文献
Abdel-Aziz, Alaa A.-M.
European Journal of Medicinal Chemistry, 2007 , vol. 42, # 5 p. 614 - 626
反应条件
in diethyl ether
T=34 - 35°C; 3 h;
参考文献
Butov; Mokhov
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 9 p. 1403 - 1404
Zh. Org. Khim., 2013 , vol. 49, # 9 p. 1419 - 1420,2
反应条件
trifluoroacetic acid
Alkylation; 12 h; Heating;
参考文献
Kazimierczuk, Zygmunt; Orzeszko, Andrzej
Helvetica Chimica Acta, 1999 , vol. 82, # 11 p. 2020 - 2027
反应条件
1: N,N-dimethyl-formamide / Reflux
2: potassium carbonate; acetone / water / 2 h / Irradiation; Inert atmosphere
View Scheme
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617
反应条件
potassium carbonate; acetone in water
2 h; IrradiationInert atmosphere; Quantum yield;
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617
反应条件
1: N,N-dimethyl-formamide / Reflux
2: water; potassium carbonate; acetone / 2 h / Irradiation; Inert atmosphere
View Scheme
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617
反应条件
1: N,N-dimethyl-formamide / Reflux
2: water; potassium carbonate; acetone / 2 h / Irradiation; Inert atmosphere
View Scheme
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617
反应条件
water; potassium carbonate; acetone
2 h; IrradiationInert atmosphere;
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617
反应条件
water; potassium carbonate; acetone
2 h; IrradiationInert atmosphere;
参考文献
Horvat, Margareta; Mlinaric-Majerski, Kata; Griesbeck, Axel G.; Basaric, Nikola
Photochemical and Photobiological Sciences, 2011 , vol. 10, # 4 p. 610 - 617