1: With potassium hexamethylsilazane in tetrahydrofuran; toluene T=-78°C; 0.5 h; Inert atmosphere; 2: With oxygen in tetrahydrofuran; toluene T=-78°C; 3: With hydrogenchloride in water T=20°C; pH=1.2;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449
2,2'-azo-bisisobutyronitrile; (tert-butyl)(2,6-dimethoxy-1-methylcyclohexa-2,5-dienyl)dimethylsilane in hexane
Giese-type addition; 14 h; Heating;
参考文献
Studer, Armido; Amrein, Stephan; Schleth, Florian; Schulte, Tobias; Walton, John C.
Journal of the American Chemical Society, 2003 , vol. 125, # 19 p. 5726 - 5733
1: (phenylsulfonyl)methane With potassium hydride in tetrahydrofuran
T=0°C; 1 h; Inert atmosphere;
2: propyl bromide in tetrahydrofuran
T=0 - 20°C; Inert atmosphere;
参考文献
Bonaparte, Amy C.; Betush, Matthew P.; Panseri, Bettina M.; Mastarone, Daniel J.; Murphy, Ryan K.; Murphree, S. Shaun
Organic Letters, 2011 , vol. 13, # 6 p. 1447 - 1449
