反应条件
1.1: lithium hexamethyldisilazane / 2-methyl cyclohexane / 3 h / 20 °C 1.2: 16 h 1.3: |Cooling with ice; |Reflux 2.1: potassium hydroxide / ethanol / 12 h / 50 °C 3.1: thionyl chloride / toluene / 2.5 h / 110 °C 4.1: N-ethyl-N,N-diisopropylamine / chloroform / 4 h / 0 - 20 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 69, p. 10 - 21
