(S)-(-)-4-苄基-5,5-二甲基-2-恶唑烷酮合成路线 (共 31 条)
反应条件
potassium carbonate in ethanol 1 h; Heating;
参考文献
Sakaguchi, Hiroshi; Tokuyama, Hidetoshi; Fukuyama, Tohru
Organic Letters, 2007 , vol. 9, # 9 p. 1635 - 1638
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; Reduction;
参考文献
Chemistry - A European Journal, , vol. 5, # 9 p. 2483 - 2491
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; 0.333333 h;
参考文献
Bull, Steven D.; Davies, Stephen G.; Nicholson, Rebecca L.; Sanganee, Hitesh J.; Smith, Andrew D.
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 16 p. 2886 - 2899
反应条件
sodium cyanoborohydride in methanol T=80°C; 5 h;
参考文献
Organic Letters, , vol. 9, # 9 p. 1635 - 1638
反应条件
in dichloromethane; ethyl acetate; Petroleum ether
参考文献
Oxford Asymmetry International plc
Patent: US5801249 A1, 1998 ;
反应条件
methanol in diethyl ether; dichloromethane T=0°C; 0.0833333 h;
参考文献
Organic Letters, , vol. 16, # 2 p. 516 - 519
反应条件
tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium in benzene T=20°C; 12 h; Inert atmosphere; optical yield given as percent dediastereoselective reaction;
参考文献
Peed, Jennifer; Davies, Iwan R.; Peacock, Lucy R.; Taylor, James E.; Kociok-Koehn, Gabriele; Bull, Steven D.
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 543 - 555
反应条件
sodium cyanoborohydride in ethanol 4 h; Heating;
参考文献
Organic Letters, , vol. 9, # 9 p. 1635 - 1638
反应条件
lithium hydroxide hydrate; dihydrogen peroxide in tetrahydrofuran; water T=0 - 20°C; 6 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 16 p. 6976 - 6979
反应条件
lithium hydroxide hydrate; dihydrogen peroxide in tetrahydrofuran; water T=0 - 20°C; 5 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 16 p. 6976 - 6979