2,3,5-三-O-(苯基甲基)-D-呋喃核糖合成路线 （共 13 条）
反应条件
acetic anhydride; dimethyl sulfoxide
T=20°C; 48 h; Inert atmosphere;
参考文献
GILEAD SCIENCES, INC.; MACKMAN, Richard, L.; PARRISH, Jay, P.; RAY, Adrian, S.; THEODORE, Dorothy, Agnes
Patent: WO2012/12776 A1, 2012 ;
Location in patent: Page/Page column 109 ;
WO 2012/012776 A1
反应条件
Multi-step reaction with 2 steps 1: NaH / dimethylformamide / 0 °C2: 0.05N HCl / dioxane / 105 °C
参考文献
Tatsuta, Kuniaki; Miura,Shozo; Ohta, Shigeru; Gunji, Hiroki Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1085 - 1088
反应条件
With tetrachloromethane; tris-(dimethylamino)-phosphine in tetrahydrofuran T=-78 - 20°C; 2.66667 h;
参考文献
Ishizuka, Takumi; Kimoto, Michiko; Sato, Akira; Hirao, Ichiro Chemical Communications, 2012 , vol. 48, # 88 p. 10835 - 10837
