2,6-二羟基-4-甲基苯甲酸甲酯合成路线 （共 2 条）
反应条件
1: SO2Cl2
View Scheme
参考文献
Dean et al.
Journal of the Chemical Society, 1956 , p. 3545,3547
反应条件
1: 74 percent / K2Co3 / dimethylformamide / Heating
2: 93 percent / t-BuOK / diisopropyl ether / Heating
3: 82 percent / DEAD, PPh3 / tetrahydrofuran
4: 45 percent / n-BuLi / tetrahydrofuran / -78 °C
5: 54 percent / PDC / dimethylformamide
6: 81 percent / Bu4(NH4), KMnO4, pyridine / dimethylformamide
7: K2CO3 / dimethylformamide
8: 81 percent / Pd(OH)2/C, cyclohexene / ethanol / Heating
View Scheme
参考文献
Ohashi, Hiroshi; Ueno, Akihiro; Nakao, Toyoo; Ito, Junko; Kimura, Kaname; Ishikawa, Masaharu; Kawai, Hiroyuki; Iijima, Hiroshi; Osawa, Tatsushi
Bioorganic and Medicinal Chemistry Letters, 1999 , vol. 9, # 14 p. 1945 - 1948
