(二甲基氨亚甲基)丙二腈合成路线 （共 23 条）
反应条件
1: 1-Imino-ethanamine hydrochloride With sodium methylate in methanol 0.166667 h; Cooling with iceLarge scale reaction; 2: α-Cyano-β-dimethylaminoacrylonitrile in methanol T=20°C; 12.5 h; CoolingLarge scale reaction;
参考文献
Zhao, Lei; Ma, Xiao-Dong; Chen, Fen-Er
Organic Process Research and Development, 2012 , vol. 16, # 1 p. 57 - 60
反应条件
in methanol T=20 - 25°C; 15.0833 h; Product distribution / selectivity;
参考文献
FUDAN UNIVERSITY; DSM IP ASSETS B.V.; CHEN, Fen-Er; MA, Xiaodong; ZHAO, Lei; XIONG, Fangjun
Patent: WO2011/60624 A1, 2011 ;
Location in patent: Page/Page column 6-7 ;
反应条件
piperidine in ethanol
3 h; Heating;
参考文献
Al-Mousawi; Mohammad; Elnagdi
Journal of Heterocyclic Chemistry, 2001 , vol. 38, # 4 p. 989 - 991
