N-对甲苯磺酰-3-吡咯啉合成路线 (共 32 条)
反应条件
N,N-bis-(mesityl)imidazolium chloride; caesium carbonate; acetylene; [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2 in toluene T=80°C; 2.5 h;
参考文献
Linnepe, Petra; Schmidt, Axel M.; Eilbracht, Peter
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 2 p. 302 - 313
反应条件
acetic acid; tris(acetonitrile)(η5-2,4-cyclopentadien-1-yl)ruthenium(1+) hexafluorophosphate(1-) T=90°C; 24 h;
参考文献
Varela, Jesus A.; Gonzalez-Rodriguez, Carlos; Rubin, Silvia G.; Castedo, Luis; Saa, Carlos
Journal of the American Chemical Society, 2006 , vol. 128, # 30 p. 9576 - 9577
反应条件
[(η6-p-cymene)RuCl(ind)(PCy3)]OTf in chlorobenzene T=20°C; 0.5 h;
参考文献
Castarlenas, Ricardo; Vovard, Chloe; Fischmeister, Cedric; Dixneuf, Pierre H.
Journal of the American Chemical Society, 2006 , vol. 128, # 12 p. 4079 - 4089
反应条件
Cu(1,1,1,5,5,5-hexafluoroacetylacetonate)2 in toluene T=110°C; 2 h;
参考文献
CORNELL RESEARCH FOUNDATION, INC.
Patent: WO2007/108999 A2, 2007 ;
Location in patent: Page/Page column 16 ;
反应条件
C31H34ClN2ORuOTf in chlorobenzene T=80°C; 4 h; Product distribution; Further Variations:Solvents;
参考文献
New Journal of Chemistry, , vol. 25, # 4 p. 519 - 521
反应条件
RuCl2(tricyclohexylphosphine)2(benzylidene); iron in toluene T=100°C; 2 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 14-15 p. 2743 - 2750,8
反应条件
sodium cyanoborohydride in trifluoroacetic acid T=20°C;
参考文献
You, Hai Tao; Grosse, Andrew C.; Howard, James K.; Hyland, Christopher J. T.; Just, Jeremy; Molesworth, Peter P.; Smith, Jason A.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 10 p. 3948 - 3953
反应条件
N,N-dicyclohexylamine; copper(I) bromide in 1,4-dioxane T=180°C; 3 h; Microwave irradiation;
参考文献
Shin, Ye Ho; Maheswara, Muchchintala; Hwang, Joon Young; Kang, Eun Joo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 11 p. 2305 - 2311
反应条件
potassium carbonate in N,N-dimethyl-formamide 1 h; Heating;
参考文献
Ohno, Hiroaki; Kadoh, Yoichi; Fujii, Nobutaka; Tanaka, Tetsuaki
Organic Letters, 2006 , vol. 8, # 5 p. 947 - 950
反应条件
Grubb's 2nd generation catalyst in water T=20°C; 3 h; Microwave irradiation;
参考文献
Lipshutz, Bruce H.; Ghorai, Subir; Aguinaldo, Grant T.
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 7-8 p. 953 - 956