L-天冬氨酸-beta-甲酯盐酸盐合成路线 (共 14 条)
参考文献
Baldwin, Jack E.; Moloney, Mark G.; North, Michael
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 833 - 834
反应条件
water in ethanol T=70°C; 2 h;
参考文献
Gmeiner; Feldman; Chu-Moyer; Rapoport
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3068 - 3074
反应条件
acetyl chloride T=5 - 10°C; Cooling with ice;
参考文献
WO2010/105367 A1, ;
Page/Page column 35; 36; 37 ;
反应条件
in methanol 1) 8-10 deg C, 3h , 2) 15 h;
参考文献
Gmeiner; Feldman; Chu-Moyer; Rapoport
Journal of Organic Chemistry, 1990 , vol. 55, # 10 p. 3068 - 3074
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 833 - 834
反应条件
lithium borohydride in tetrahydrofuran
参考文献
Carbohydrate research, , vol. 47, # 1 p. 35 - 48
反应条件
ammonia in tetrahydrofuran; methanol; diethyl ether T=25°C; 96 h;
参考文献
Gani, David; Young, Douglas W.; Carr, David M.; Poyser, J. Philip; Sadler, Ian H.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 11 p. 2811 - 2814
反应条件
sodium carbonate in 1,4-dioxane Ambient temperature;
参考文献
Kadota, Isao; Saya, Shioko; Yamamoto, Yoshinori
Heterocycles, 1997 , vol. 46, # 1 p. 335 - 348
反应条件
di-tert-butyl dicarbonate; sodium carbonate in 1,4-dioxane; water T=0 - 20°C;
参考文献
Ollivier, Anthony; Goubert, Marlene; Tursun, Ahmatjan; Canet, Isabelle; Sinibaldia, Marie-Eve
Arkivoc, 2010 , vol. 2010, # 9 p. 108 - 126
反应条件
1: With water; sodium carbonate in 1,4-dioxane T=5 - 20°C; Cooling with ice; 2: With hydrogenchloride in 1,4-dioxane; water
参考文献
VALORISATION-RECHERCHE SOCIETE EN COMMANDITE; LUBELL, William; JAMIESON, Andrew; BOUTARD, Nicolas; RONGA, Luisa; ST-CYR, Daniel; TURCOTTE, Daniel; CHEN, Wang
Patent: WO2010/105367 A1, 2010 ;
Location in patent: Page/Page column 35; 36; 37 ;