反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; benzene byproducts: NaI; ethanolic soln. of iodocarborane addn. to benzene soln. PhB(OH)2 and Pd-compd. and aq. soln. of Na2CO3 (vigorous stirring, Ar-atmosphere), boiling (18 h, 65-70°C), Na2CO3 addn., boiling (23 h), further addn. of Pd-compd., boiling (24 h); mixture cooling, extracting (Et2O), extracts washing (saturated NaCl soln.), drying (Na2SO4), solvent removing, sepn. by column chromy.; identification by GLC;
参考文献
Russian Journal of General Chemistry, , vol. 68, # 6 p. 922 - 924
