4,4,4-三苯基-1-丁烯合成路线 （共 26 条）
反应条件
1: (i) NaBH4, H2SO4, (ii) aq. H2O2, aq. NaOH 2: Pb(OAc)4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 33, # 7 p. 2767 - 2774
反应条件
tris(pentafluorophenyl)-borane in dichloromethane
T=20°C;
参考文献
Rubin, Michael; Gevorgyan, Vladimir
Organic Letters, 2001 , vol. 3, # 17 p. 2705 - 2707
反应条件
InOTf in dichloromethane
T=25°C; 0.5 h; Inert atmosphere;
参考文献
Dao, Hai Thanh; Schneider, Uwe; Kobayashi, Shu
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2522 - 2529
反应条件
anhydrous iron chloride in dichloromethane
T=20°C; 6.5 h;
参考文献
Fan, Xiaohui; Cui, Xiao-Meng; Guan, Yong-Hong; Fu, Lin-An; Lv, Hao; Guo, Kun; Zhu, Hong-Bo
European Journal of Organic Chemistry, 2014 , vol. 2014, # 3 p. 498 - 501
反应条件
triphenylphosphine in benzene
T=60°C; 1.5 h;
参考文献
Reid, Simon J.; Baird, Michael C.
Journal of the Chemical Society. Dalton Transactions, 2003 , # 20 p. 3975 - 3980
反应条件
tin(IV) chloride in dichloromethane
T=25°C; 68 h;
参考文献
Mayr, Herbert; Gorath, Gorden; Bauer, Bernhard
Angewandte Chemie, 1994 , vol. 106, # 7 p. 793 - 794
反应条件
dichloro(cycloocta-1,5-diene)palladium(II); potassium hexamethylsilazane; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in ethylene glycol dimethyl ether
T=24°C; 12 h; Inert atmosphere;
参考文献
Sha, Sheng-Chun; Zhang, Jiadi; Carroll, Patrick J.; Walsh, Patrick J.
Journal of the American Chemical Society, 2013 , vol. 135, # 46 p. 17602 - 17609
反应条件
chloro-trimethyl-silane; benzaldehyde in dichloromethane
Ambient temperature;
参考文献
Chen, Chien-Tien; Chao, Shi-Deh
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1090 - 1091
反应条件
titanium tetrachloride in dichloromethane
42 h; Ambient temperature;
参考文献
Nozaki, Kyoko; Nanno, Tetsuo; Takaya, Hidemasa
Journal of Organometallic Chemistry, 1997 , vol. 527, # 1-2 p. 103 - 108
反应条件
triphenylphosphine in benzene
T=60°C; Substitution; Isomerization; Title compound not separated from byproducts.;
参考文献
Reid; Freeman; Baird
Chemical Communications, 2000 , # 18 p. 1777 - 1778
