5-氟-3-硝基-2-甲基苯胺合成路线 (共 5 条)
反应条件
Na2S*9H2O in ethanol; water
参考文献
US5916900 A1, ;
US 5916900 A
反应条件
Na2S*9H2O in ethanol; water
参考文献
US5576437 A1, ;
US 5576437 A
反应条件
sulfuric acid; nitric acid in hexane; ethyl acetate
参考文献
US5576437 A1, ;
US 5576437 A
反应条件
1: nitric acid; sulfuric acid / 3 h / -5 - 20 °C 2: Na2S*9H2O / ethanol; water / 2.5 h / 20 °C View Scheme
反应条件
sodium nitrate; acetic acid T=4 - 20°C;
参考文献
MERCK SHARP and DOHME CORP.; CERNAK, Timothy, A.; DYKSTRA, Kevin, D.; SHEN, Dong-Ming; LIU, Kun; STAMFORD, Andrew; TAN, John Qiang
Patent: WO2014/14794 A2, 2014 ;
Location in patent: Page/Page column 80 ;