2-溴-4,6-二甲基嘧啶合成路线 （共 4 条）
反应条件
in benzonitrile T=100°C; 20 h;
参考文献
Mikhailov, A. S.; Pashkurov, N. G.; Reznik, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 12 p. 2304 - 2307
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 12 p. 2767 - 2771
反应条件
1: 1.7 g / 170 - 200 °C / 15 Torr 2: 1.1 g / Na / methanol View Scheme
参考文献
Mikhailov, A. S.; Pashkurov, N. G.; Reznik, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 12 p. 2304 - 2307
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 12 p. 2767 - 2771
反应条件
T=165 - 205°C; P=15 Torr; Further byproducts given;
参考文献
Mikhailov, A. S.; Pashkurov, N. G.; Reznik, V. S.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 12 p. 2304 - 2307
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 12 p. 2767 - 2771
反应条件
n-butyllithium in diethyl ether; pentane
T=-90 - 20°C; Formylation; 1.5 h;
参考文献
Barr, Christa L.; Chase, Preston A.; Hicks, Robin G.; Lemaire, Martin T.; Stevens, Cecilia L.
Journal of Organic Chemistry, 1999 , vol. 64, # 24 p. 8893 - 8897
