反应条件
in ethanol
anhydrous ethanol; addn. Et3N to ligand soln., dropwise addn. chloride soln., heating under reflux for 8 h, concn. (pptn.); washing (cold EtOH, ether), recrystn. (EtOH/ether = 1:5); elem. anal.;
参考文献
Gang, Zhao; Yuan, Cao
Synthesis and Reactivity in Inorganic and Metal-Organic Chemistry, 1995 , vol. 25, p. 1207 - 1217
