(2-溴-3-甲基苯基)甲醇合成路线 (共 2 条)
反应条件
1: With chloroformic acid ethyl ester; triethylamine in tetrahydrofuran 0.25 h; Cooling with ice; 2: With sodium tetrahydroborate; water in tetrahydrofuran Cooling with ice;
参考文献
AMGEN INC.; PARAS, Nick A,; BROWN, James; CHENG, Yuan; HITCHCOCK, Stephen; JUDD, Ted; LOPEZ, Patricia; MINATTI, Ana Elena; NIXEY, Thomas; POWERS, Timothy; TEGLEY, Christopher M.; XUE, Qiufen; YANG, Bryant; ZHONG, Wenge
Patent: WO2011/90911 A1, 2011 ;
Location in patent: Page/Page column 54; 55 ;
WO 2011/090911 A1
反应条件
manganese(IV) oxide in chloroform
参考文献
AJINOMOTO CO., INC.
Patent: US2011/82109 A1, 2011 ;
Location in patent: Page/Page column 33 ;
US 20110082109 A1