2,6-二异丙基-5,5-二甲基-1,3-二恶烷-4-醇合成路线 (共 6 条)
反应条件
cesium fluoride T=20°C; 1.5 h;
参考文献
Chuit, C.; Corriu, R. J. P.; Reye, C.
Synthesis, 1983 , # 4 p. 294 - 297
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; isopropyl (diphenylmethylsilyl)acetate; lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; Yield given. Yields of byproduct given;
参考文献
Larson, Gerald L.; Quiroz, Fernando; Suarez, Juan
Synthetic Communications, 1983 , vol. 13, # 10 p. 833 - 844
参考文献
Saunders; Murray; Cleveland
Journal of the American Chemical Society, 1943 , vol. 65, p. 1715
参考文献
Hine et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 1184,1187
反应条件
water; nickel T=50 - 85°C; Hydrogenation;
参考文献
Hagemeyer et al.
Preprints - American Chemical Society, Division of Petroleum Chemistry, 1956 , vol. 1, # 2 p. 63,65
反应条件
acetic acid
Abdestillieren des entstehenden Isobutyraldehyds;
参考文献
Hagemeyer et al.
Preprints - American Chemical Society, Division of Petroleum Chemistry, 1956 , vol. 1, # 2 p. 63,65