反应条件
triethylamine in diethyl ether
byproducts: 3,5-diisopropylidene-1,2,4-trithiolane, (HNEt3)Cl; stirring (-30°C, 1 h, 20°C, 3 h); filtration, concn. (vac.), solidification by addn. of a small amt. of hexane, elimination of the byproduct by repeated pptn. from hexane; analytically not pure;
参考文献
Hartke, Klaus; Wagner, Uwe
Chemische Berichte, 1996 , vol. 129, # 6 p. 663 - 669
