in dichloromethane-d2
N2-atmosphere; 1 equiv. MeI, 5 min; not isolated, detd. by NMR spectroscopy;
参考文献
Janzen, Michael C.; Jenkins, Hilary A.; Rendina, Louis M.; Vittal, Jagadese J.; Puddephatt, Richard J.
Inorganic Chemistry, 1999 , vol. 38, # 9 p. 2123 - 2130
in benzene
byproducts: Me3SiCl; absence of air and moisture; simultaneous dropping of benzene solns. of equimolar amts. of Sn-compd. and S(SiMe3)2 into benzene, stirring (overnight, pptn.); filtration (after 10 days), washing (C6H6), sublimation (vac.);
参考文献
Jenkins, Linda S.; Wiley, Gerald R.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1979 , p. 1697 - 1700
in diethyl ether
byproducts: CH3OH; treating with moist ether, sepn. of NaCl and S, filtrate evapn. in vacuum; ppt. washing (hot water), Sn-compd. remaining on the filtration paper, N-compd. pptn. on cooling (5°C), residue insoluble in ether were Sn-containing sulfite and Sn-containing sulfate; IR spectroscopy;
参考文献
Shcherbakov; Basova
Russian Journal of General Chemistry, 1997 , vol. 67, # 7 p. 1049 - 1053
