反应条件
in sulfur dioxide exclusion of air and moisture; 1. method: NMR-tube; SO2 and SbF5 alternate condensed to KPHF5 at 77 K; melted off; shake at 205 K; 2.method: react. in two leg vessel; 1.method: KSbF6 pptd.; NMR-spectroscopy; 2.method: pptn. separated; solvent removed; Raman-spectroscopy of residue;
参考文献
Zeitschrift fuer Naturforschung, B: Chemical Sciences, , vol. 44, # 6 p. 679 - 682
