1: AlCl3 / toluene / 1 h / 50 - 60 °C / or benzene 2: diethyl ether 3: 0.5 g / P2O5, H3PO4 / 3 h / 100 °C 4: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
1: 1.) KCN 2.) conc. HCl, AcOH / 1.) H2O, EtOH, room temperature, 6 days 2.) reflux, 72 h 2: acetanhydride / 6 h / Heating 3: AlCl3 / toluene / 1 h / 50 - 60 °C / or benzene 4: diethyl ether 5: 0.5 g / P2O5, H3PO4 / 3 h / 100 °C 6: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
1: acetanhydride / 6 h / Heating 2: AlCl3 / toluene / 1 h / 50 - 60 °C / or benzene 3: diethyl ether 4: 0.5 g / P2O5, H3PO4 / 3 h / 100 °C 5: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
1: 1 g / AlCl3 / petroleum ether / 1.) room temperature, 3 h 2.) 65-70 deg C, 1 h 2: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
1: 0.5 g / P2O5, H3PO4 / 3 h / 100 °C 2: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
1: 60 percent 2: 1.) KCN 2.) conc. HCl, AcOH / 1.) H2O, EtOH, room temperature, 6 days 2.) reflux, 72 h 3: acetanhydride / 6 h / Heating 4: AlCl3 / toluene / 1 h / 50 - 60 °C / or benzene 5: diethyl ether 6: 0.5 g / P2O5, H3PO4 / 3 h / 100 °C 7: 0.8 g / LAH / tetrahydrofuran / Heating View Scheme
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
palladium on activated charcoal T=360 - 380°C; 24 h;
参考文献
Mitra, Ashutosh; Ray, Rebati M.; Majumder, Arun K.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 449 - 452
