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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
169178-80-7
合成路线
(共 8 条)
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
4900-62-3
+
169178-80-7
反应条件
in dichloromethane T=20°C; 1 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola; Robinson, Ward T.
Acta Chemica Scandinavica, 1995 , vol. 49, # 4 p. 253 - 264
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
169178-80-7
反应条件
in dichloromethane T=-50°C; 0.5 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola; Robinson, Ward T.
Acta Chemica Scandinavica, 1995 , vol. 49, # 4 p. 253 - 264
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
4900-62-3
+
13041-62-8
4-甲氧基-1-萘甲酸
+
169178-80-7
反应条件
in dichloromethane T=20°C; 2 h; Irradiation; Further byproducts given;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola; Robinson, Ward T.
Acta Chemica Scandinavica, 1995 , vol. 49, # 4 p. 253 - 264
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
4900-62-3
+
169178-80-7
反应条件
in dichloromethane T=20°C; 1 h; Irradiationvar. temp. and time reaction; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola; Robinson, Ward T.
Acta Chemica Scandinavica, 1995 , vol. 49, # 4 p. 253 - 264
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
19817-09-5
+
4900-62-3
+
51934-42-0
+
169178-80-7
反应条件
in ethanol; acetonitrile T=20°C; 1 h; Irradiationthe effect of ethanol; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 718 - 732
509-14-8
四硝基甲烷
+
2216-69-5
1-甲氧基萘
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
19817-09-5
+
51934-42-0
+
169178-80-7
反应条件
in ethanol; dichloromethane T=20°C; 1 h; Irradiationthe effects of ethanol, dark storage, and reaction time; Product distribution;
参考文献
Butts, Craig P.; Eberson, Lennart; Hartshorn, Michael P.; Persson, Ola
Acta Chemica Scandinavica, 1997 , vol. 51, # 6-7 p. 718 - 732
169178-80-7
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
13041-62-8
4-甲氧基-1-萘甲酸
反应条件
α-naphthyl methyl ether in dichloromethane T=22°C; 150 h; various solvents, additives, reaction circumstances (irrad.); monitored by UV, NMR, FTIR and EPR spectroscopy; Rate constantMechanism;
参考文献
Eberson, Lennart; Hartshorn, Michael P.; Radner; Svensson, Jan Olof
Acta Chemica Scandinavica, 1996 , vol. 50, # 10 p. 885 - 898
169178-80-7
→
反应条件
4900-63-4
1-甲氧基-4-硝基萘
+
13041-62-8
4-甲氧基-1-萘甲酸
反应条件
α-naphthyl methyl ether in dichloromethane T=22°C; 150 h; various solvents, additives, reaction circumstances (irrad.); monitored by UV, NMR, FTIR and EPR spectroscopy; Rate constantMechanism;
参考文献
Acta Chemica Scandinavica, , vol. 50, # 10 p. 885 - 898