反应条件
in hexane
mixt. heated at 60°C for 12 h; pptd. at -60°C for 6 h, filtered off, washed with pentane at -78°C; or evapd., distd. at 95-115°C at 0.1 Torr, oil crystd.after 5 d, recrystd. (pentane at -78°C); elem. anal.;
参考文献
Wrackmeyer, Bernd
Organometallics, 1984 , vol. 3, p. 1 - 4
