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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
吡啶-3-硼酸
合成路线
（共 163 条）
461425-63-8
3-溴-4-乙基苯甲醛
+
1692-25-7
吡啶-3-硼酸
→
反应条件
628711-66-0
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in toluene T=80°C; 16 h; Nitrogen atmosphere;
参考文献
AMGEN INC.
Patent: WO2003/99776 A1, 2003 ;
Location in patent: Page 108-109 ;
612-62-4
2-氯喹啉
+
1692-25-7
吡啶-3-硼酸
→
反应条件
6294-65-1
反应条件
Na2[PdCl4]; cataCXium FSulf; potassium carbonate in water; butan-1-ol T=100°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Fleckenstein, Christoph A.; Plenio, Herbert
Chemistry - A European Journal, 2008 , vol. 14, # 14 p. 4267 - 4279
59-31-4
2-羟基喹啉
+
1692-25-7
吡啶-3-硼酸
→
反应条件
6294-65-1
反应条件
1: 2-hydroxyquinoline With potassium carbonate; bromo-tris(1-pyrrolidinyl)phosphonium hexafluorophosphate in 1,4-dioxane T=100°C; 3 h; Inert atmosphere; 2: pyridin-3-yl boronic acid With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in 1,4-dioxane; water T=100°C; Suzuki-Miyaura coupling; Inert atmosphere;
参考文献
Li, Shui-Ming; Huang, Jie; Chen, Guo-Jun; Han, Fu-She
Chemical Communications, 2011 , vol. 47, # 48 p. 12840 - 12842
2005-43-8
2-溴喹啉
+
1692-25-7
吡啶-3-硼酸
→
反应条件
6294-65-1
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate T=80°C; Suzuki cross-coupling;
参考文献
Voets, Marieke; Antes, Iris; Scherer, Christiane; Mueller-Vieira, Ursula; Biemel, Klaus; Barassin, Catherine; Marchais-Oberwinkler, Sandrine; Hartmann, Rolf W.
Journal of Medicinal Chemistry, 2005 , vol. 48, # 21 p. 6632 - 6642
1692-25-7
吡啶-3-硼酸
→
反应条件
5094-12-2
2-甲基-2,3,4,5-四氢-1H-吡啶并[4,3-b]吲哚
反应条件
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / 1,4-dioxane; water / 2.5 h / 80 °C / Inert atmosphere 2.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere 2.2: 0 - 20 °C / Inert atmosphere 3.1: dichloromethane / 20 °C / Inert atmosphere 4.1: ruthenium(III) chloride polyhydrate / isopropanol acetate / 15 h / 80 °C / Inert atmosphere 5.1: sodium tetrahydroborate / methanol; water / 20 - 100 °C / Inert atmosphere View Scheme
参考文献
Dong, Huijun; Latka, Regina T.; Driver, Tom G.
Organic Letters, 2011 , vol. 13, # 10 p. 2726 - 2729
1692-25-7
吡啶-3-硼酸
→
反应条件
64368-85-0
8-氟-2-甲基-2,3,4,5-四氢-1H-吡啶并[4,3-b]吲哚
反应条件
1.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / 1,4-dioxane; water / 2.5 h / 80 °C / Inert atmosphere 2.1: acetic acid; sodium nitrite / water / 1.5 h / 0 °C / Inert atmosphere 2.2: 0 - 20 °C / Inert atmosphere 3.1: dichloromethane / 20 °C / Inert atmosphere 4.1: ruthenium(III) chloride polyhydrate / isopropanol acetate / 15 h / 80 °C / Inert atmosphere 5.1: sodium tetrahydroborate / methanol; water / 20 - 100 °C / Inert atmosphere View Scheme
参考文献
Dong, Huijun; Latka, Regina T.; Driver, Tom G.
Organic Letters, 2011 , vol. 13, # 10 p. 2726 - 2729
1899-24-7
5-溴-2-呋喃甲醛
+
1692-25-7
吡啶-3-硼酸
→
反应条件
38588-49-7
5-吡啶-3-基-2-糠醛
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether T=90°C; Suzuki coupling; 1 h;
参考文献
Yano, Jason K.; Denton, Travis T.; Cerny, Matthew A.; Zhang, Xiaodong; Johnson, Eric F.; Cashman, John R.
Journal of Medicinal Chemistry, 2006 , vol. 49, # 24 p. 6987 - 7001
1072-98-6
2-氨基-5-氯吡啶
+
1692-25-7
吡啶-3-硼酸
→
反应条件
39883-47-1
[2,3-联吡啶]-6-胺
反应条件
SS-Phos; palladium diacetate; potassium carbonate in water T=100°C; Suzuki-Miyaura coupling; 12 h;
参考文献
Anderson, Kevin W.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2005 , vol. 44, # 38 p. 6173 - 6177
19798-81-3
2-氨基-6-溴吡啶
+
1692-25-7
吡啶-3-硼酸
→
反应条件
39883-47-1
[2,3-联吡啶]-6-胺
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine; potassium carbonate in N,N-dimethyl acetamide; butan-1-ol T=110°C; Suzuki Coupling; 24 h; Inert atmosphere;
参考文献
Wang, Kun; Fu, Qi; Zhou, Rong; Zheng, Xueli; Fu, Haiyan; Chen, Hua; Li, Ruixiang
Applied Organometallic Chemistry, 2013 , vol. 27, # 4 p. 232 - 238
45644-21-1
2-氨基-6-氯吡啶
+
1692-25-7
吡啶-3-硼酸
→
反应条件
39883-47-1
[2,3-联吡啶]-6-胺
反应条件
bis(η3-allyl-μ-chloropalladium(II)); N,N,N′,N′-tetra(diphenylphosphinomethyl)-1,2-ethylenediamine; potassium carbonate in N,N-dimethyl acetamide; butan-1-ol T=110°C; Suzuki Coupling; 20 h; Inert atmosphere;
参考文献
Wang, Kun; Fu, Qi; Zhou, Rong; Zheng, Xueli; Fu, Haiyan; Chen, Hua; Li, Ruixiang
Applied Organometallic Chemistry, 2013 , vol. 27, # 4 p. 232 - 238
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