甲基丙烯酸-2-羟-3-苯氧基丙酯合成路线 (共 4 条)
反应条件
sodium hydroxide; 2,6-di-tert-butyl-4-methyl-phenol; triethylamine in dichloromethane
参考文献
SEPTODONT CONFI-DENTAL DIVISION
Patent: US2010/307378 A1, 2010 ;
反应条件
2,6-di-tert-butyl-4-methyl-phenol; triethylamine T=60°C; 24 h; Inert atmosphere;
参考文献
Septodont Confi-Dental; Trujillo-Lemon, Marianela; Wall, Kristin Lindsay; Esquibel, Kristina; Boulden, Jordan; Docktor, Amy J.; Shelton, Zachary R.; Bracho-Troconis, Cora
Patent: US8513326 B2, 2013 ;
Location in patent: Page/Page column 30; 31 ;
反应条件
1: phenolated sodium With Amberlite IRA-400 resin in water 2: methacrylic acid 2,3-epoxypropyl ester in ethanol T=50°C; 1.5 h;
参考文献
Tamami; Iranpoor; Rezaei
Synthetic Communications, 2004 , vol. 34, # 15 p. 2789 - 2795
反应条件
chromium (III) ethanoate 80 h; Kinetics;
参考文献
Bukowska, Agnieszka; Bukowski, Wiktor
Organic Process Research and Development, 1999 , vol. 3, # 6 p. 432 - 436