4-苯胺-3-硝基苯甲酸合成路线 （共 10 条）
反应条件
1: in ethanol 16 h; Reflux; 2: With hydrogenchloride in ethanol; water
参考文献
Sumitomo Chemical Company, Limited
Patent: EP2436683 A1, 2012 ;
Location in patent: Page/Page column 43 ;
反应条件
potassium carbonate in water T=150°C; 2 h;
参考文献
Lan, Cong; Xia, Zhi-Ning; Li, Zheng-Hua; Liang, Rong-Hui
Journal of Chemical Research, 2012 , vol. 36, # 12 p. 726 - 728
反应条件
1: nitric acid / 1 h / Heating 2: propan-1-ol / 12 h / Reflux View Scheme
参考文献
Asian Journal of Chemistry, , vol. 23, # 4 p. 1569 - 1572
反应条件
1: sulfuric acid; chromic acid / 30 - 50 °C 2: potassium carbonate View Scheme
参考文献
Helvetica Chimica Acta, , vol. 26, p. 475,480
参考文献
Helvetica Chimica Acta, , vol. 26, p. 475,480
参考文献
Chemische Berichte, , vol. 22, p. 3287
Chemische Berichte, , vol. 23, p. 1842
反应条件
1.1: hydrogen / palladium 10 on activated carbon / tetrahydrofuran / 2.5 h / 20 °C 2.1: hydrogenchloride / toluene / 2.75 h / Reflux 2.2: 20 °C 2.3: 5 - 10 °C / pH ~ 4 View Scheme
参考文献
Sumitomo Chemical Company, Limited
Patent: EP2436683 A1, 2012 ;
反应条件
1: HCl(g) / 18 h / Heating 2: H2 / 5 percent Pd/C / methanol; ethyl acetate 3: 2-methoxy-ethanol / 3 h / Heating View Scheme
参考文献
Palmer, Brian D.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 27 p. 5457 - 5465
反应条件
1: alcoholic ammonium sulfide / 120 °C / im Einschlussrohr 2: beim Erhitzen ueber den Schmelzpunkt View Scheme
参考文献
Schoepff
Chemische Berichte, 1889 , vol. 22, p. 3287
Chemische Berichte, 1890 , vol. 23, p. 1842
反应条件
hydrogen; palladium 10 on activated carbon in tetrahydrofuran
T=20°C; 2.5 h;
参考文献
Sumitomo Chemical Company, Limited
Patent: EP2436683 A1, 2012 ;
Location in patent: Page/Page column 44 ;
