1-(3,4-亚甲基二氧基苯基)丁烷合成路线 （共 6 条）
反应条件
methanol; palladium 10 on activated carbon; hydrogen; potassium carbonate T=65°C; P=760.051 Torr; 24 h; Catalytic behavior;
参考文献
Tetrahedron, , vol. 69, # 30 p. 6083 - 6087
反应条件
1: With magnesium Grignard reaction; 2: With hydrogen; palladium on activated charcoal Hydrogenation;
参考文献
Sidhu; Marcus; Parkinson; Omiecinski
Journal of biochemical and molecular toxicology, 1998 , vol. 12, # 5 p. 253 - 262
反应条件
in tetrahydrofuran 1) -80 deg C, , 2 min, 2) 10 min, 3) 25 deg C, 45 min;
参考文献
Sanghvi, Y. S.; Dabral, V.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 9 p. 893
反应条件
1: methanol / 60 °C / |Inert atmosphere 2: potassium carbonate; methanol; hydrogen; palladium 10 on activated carbon / 24 h / 65 °C / 760.05 Torr View Scheme
参考文献
Tetrahedron, , vol. 69, # 30 p. 6083 - 6087
反应条件
n-butyllithium 1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Yield given. Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 23, # 1 p. 12 - 14
反应条件
n-butyllithium 1) in hexane, tetrahydrofuran, -78 deg C, 5 min 2) 0.5 h, -78 deg C, then -10 deg C; Multistep reaction. Further byproducts given. Title compound not separated from byproducts;
参考文献
Sanghvi, Y. S.; Dabral, V.; Bhat, K. S.; Rao, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 1 p. 12 - 14
