(4-噻吩-2-苯基)甲醇合成路线 (共 55 条)
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; silver(l) oxide in methanol T=20°C; Suzuki-Miyaura cross- coupling; 1.5 h; Inert atmosphere;
参考文献
Australian Journal of Chemistry, , vol. 61, # 11 p. 870 - 873
反应条件
1: (4-Methylphenyl)-magnesium bromide With bismuth(III) chloride 2: thien-2-yl bromide With potassium phosphate; palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 1 h; Inert atmosphere;
参考文献
Synlett, , # 9 p. 1324 - 1330
反应条件
C52H44CoN4O4; potassium hydroxide; tert-butyl alcohol T=200°C; 10 h; Inert atmosphereDarkness;
参考文献
Tetrahedron Letters, , vol. 53, # 13 p. 1571 - 1575
反应条件
tris-(dibenzylideneacetone)dipalladium(0); copper(I) bromide dimethylsulfide complex; trifuran-2-yl-phosphane in tetrahydrofuran Stille coupling; Heating;
参考文献
Journal of the American Chemical Society, , vol. 125, # 50 p. 15292 - 15293
反应条件
copper(l) iodide; sodium pentafluorophenolate in various solvent(s) T=130°C; 12 h;
参考文献
Chemistry Letters, , # 7 p. 639 - 640
反应条件
tetrakis(triphenylphosphine) palladium(0) T=80°C; Stille cross-coupling; 20 h; Ionic liquidInert atmosphere;
参考文献
Synthetic Communications, , vol. 42, # 16 p. 2396 - 2406
反应条件
trifluoroacetic acid T=65 - 70°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 50, # 13 p. 2232 - 2235
反应条件
PEPPSI™-IPr catalyst; cesium fluoride in 1,4-dioxane T=20 - 60°C; Stille-Migita cross-coupling; 24 h; Molecular sieveInert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 16, # 14 p. 4279 - 4283
反应条件
[Ni(1-(1-ethyl-benzimidazol-2-ylmethyl)-3-mesitylimidazolin-2-ylidene)2][Cl]2; sodium acetate in tetrahydrofuran T=20°C; Kumada-Corriu coupling reaction; Inert atmosphere;
参考文献
Dalton Transactions, , vol. 39, # 22 p. 5231 - 5241
反应条件
2,6-diiodo-BODIPY in dimethyl sulfoxide T=20°C; 1 h; Inert atmosphereIrradiation; Catalytic behavior; Reagent/catalyst;
参考文献
RSC Advances, , vol. 3, # 45 p. 23377 - 23388