反式-1-苯基-1,3-丁二烯合成路线 (共 179 条)
反应条件
Multistep reaction.;
参考文献
Chemistry - A European Journal, , vol. 10, # 1 p. 101 - 108
反应条件
1: CH2Cl2 / 1 h / Ambient temperature 2: 76 percent / NaBH4 / diethyl ether / 2 h / 10 - 20 °C 3: 75 percent / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 19 p. 3791 - 3794
反应条件
tetrakis(triphenylphosphine) palladium(0) in ethyl acetate T=20°C; Suzuki-Miyaura-type reaction; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 15, # 45 p. 12247 - 12254
反应条件
1: pyridine / dichloromethane / 15 h / 0 °C / Reflux; Inert atmosphere 2: [Ni0(1,5-cyclooctadiene)2]; tri(2-methoxy-phenyl)-phosphine; triethylsilyl trifluoromethanesulphonate; triethylamine / toluene / 20 °C / 760.05 Torr / Inert atmosphere View Scheme
参考文献
Chemistry - An Asian Journal, , vol. 6, # 7 p. 1860 - 1875
反应条件
NiCl2((PPh3)P)2 in benzene 16 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 56, # 18 p. 5289 - 5293
反应条件
Carbowax 6000 (liquid); potassium carbonate T=150°C; P=15 Torr; Yield given. Yields of byproduct given;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 6 p. 269 - 271
反应条件
iron(III) chloride; potassium carbonate in tetrahydrofuran; diethyl ether T=10 - 15°C; 18 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , p. 2157 - 2167
Zhurnal Organicheskoi Khimii, , vol. 19, # 12 p. 2465 - 2477
反应条件
potassium carbonate in toluene Heating;
参考文献
Organic and Biomolecular Chemistry, , vol. 6, # 8 p. 1344 - 1348
反应条件
Multistep reaction.;
参考文献
Chemistry - A European Journal, , vol. 10, # 1 p. 101 - 108
反应条件
1: 83 percent / tetrahydrofuran / 1 h / -78 °C 2: KH / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Synthesis, , # 9 p. 1223 - 1228