反式-1-苯基-1,3-丁二烯合成路线 （共 179 条）
反应条件
in toluene T=110°C; 72 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 53, # 2 p. 251 - 258
反应条件
in toluene T=110°C; 72 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ono, Noboru; Kamimura, Akio; Kaji, Aritsune
Journal of Organic Chemistry, 1988 , vol. 53, # 2 p. 251 - 258
反应条件
sulfur T=340°C; P=300 Torr;
参考文献
Journal of Organic Chemistry, , vol. 14, p. 761,768
Zhurnal Obshchei Khimii, , vol. 19, p. 1356,1362
Chem.Abstr., , p. 1955
反应条件
oxygen O2, singlet; rose bengal in methanol; dichloromethane T=15 - 17°C; 21 h; Irradiation;
参考文献
Tetrahedron, , vol. 41, # 11 p. 2147 - 2154
反应条件
1: 30 percent / O2; rose bengal, bis(triethylammonium)salt / CH2Cl2 / 6 h / 5 - 10 °C / Irradiation 2: 85 percent / Et3N; PPh3 / CH2Cl2 / 2 h / 20 °C 3: 100 percent / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 18 p. 5531 - 5546
反应条件
1.1: Pt(dibenzylideneacetone)3; (3R,5R)-5-(tert-butyl)-2,2-diisobutyl-3-phenyl-1,3-oxaphospholane; 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane / toluene / 12 h / 60 °C / Inert atmosphere 1.2: 0 - 20 °C / Inert atmosphere 2.1: ozone / methanol; dichloromethane / -78 °C View Scheme
参考文献
Schuster, Christopher H.; Li, Bo; Morken, James P.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 34 p. 7906 - 7909
反应条件
2: palladium/charcoal / 300 °C 3: H2SO4 View Scheme
参考文献
McBee et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 3389
Journal of Organic Chemistry, 1956 , vol. 38, p. 632
反应条件
hydrogen; [rhodium(I)(carbonyl)2(acetylacetonate)]; (R,S)-binaphos in benzene T=30°C; P=76000 Torr; 48 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Horiuchi, Toshihide; Ohta, Tetsuo; Nozaki, Kyoto; Takaya, Hidemasa
Chemical Communications, 1996 , # 2 p. 155 - 156
反应条件
[rhodium(I)(carbonyl)2(acetylacetonate)]; hydrogen; (R,S)-Binaphos in benzene T=30°C; P=30400 Torr; 24 h;
参考文献
Horiuchi, Toshihide; Ohta, Tetsuo; Shirakawa, Eiji; Nozaki, Kyoko; Takaya, Hidemasa
Tetrahedron, 1997 , vol. 53, # 23 p. 7795 - 7804
反应条件
1: CCl3CO2H / benzene 2: Na2Cr2O7, aq. H2SO4 / acetic acid View Scheme
参考文献
House,H.O. et al.
Journal of Organic Chemistry, 1972 , vol. 37, p. 1003 - 1011
