反式-1-苯基-1,3-丁二烯合成路线 (共 179 条)
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; acetic acid in tetrahydrofuran T=80°C; 4 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 15 p. 3809 - 3810
反应条件
sodium tetrahydroborate in methanol; diethyl ether T=10 - 20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 40, # 19 p. 3791 - 3794
反应条件
pinacol borane; triethylamine; bis[2-(diphenylphosphino)phenyl] ether; palladium diacetate in tetrahydrofuran; 1,4-dioxane T=100°C; 5 h;
参考文献
Tetrahedron, , vol. 63, # 45 p. 10939 - 10948
反应条件
bis(η3-allyl-μ-chloropalladium(II)); TASF-(Et); triethyl phosphite in tetrahydrofuran T=50°C;
参考文献
Journal of Organic Chemistry, , vol. 53, # 4 p. 918 - 920
反应条件
triethylamine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in propan-1-ol Suzuki cross-coupling reaction; 3 h; Heating;
参考文献
Organic Letters, , vol. 4, # 1 p. 107 - 109
反应条件
indium(III) chloride; indium; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=20°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 1 p. 180 - 182
反应条件
1: With dibutylzirconocene in tetrahydrofuran; hexane T=-78 - 20°C; 2: With hydrogenchloride in tetrahydrofuran; hexane T=20°C; Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 125, # 43 p. 13258 - 13264
反应条件
T=700°C; P=0.01 Torr; flash vacuum pyrolysis;
参考文献
Journal of Organic Chemistry, , vol. 45, # 20 p. 4065 - 4067
反应条件
(IMes)CuCl; triphenylphosphine; isopropyl alcohol in 1,4-dioxane; diethyl ether T=60°C; 2 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 1 p. 144 - 149
反应条件
water; palladium diacetate; triphenylphosphine in tetrahydrofuran T=50°C; Suzuki-Miyaura Coupling; 24 h; stereoselective reaction;
参考文献
Organic Letters, , vol. 14, # 1 p. 390 - 393