反式-1-苯基-1,3-丁二烯合成路线 (共 179 条)
反应条件
triethylammonium phosphinate; tris(triphenylphosphine)ruthenium(II) chloride T=40°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 37, # 36 p. 6599 - 6602
反应条件
titanium(IV) isopropylate; manganese(IV) oxide; 1-methyl-1,5,7-triazabicyclo[4.4.0]dec-5-ene in tetrahydrofuran oxidation-Wittig reaction; 48 h; Heating;
参考文献
Synlett, , # 2 p. 215 - 218
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran T=-60°C; 2: With dihydrogen peroxide in tetrahydrofuran; water T=0 - 20°C; 1.33333 h;
参考文献
Tetrahedron Letters, , vol. 43, # 31 p. 5495 - 5497
反应条件
Mo(CO)3(CN-t-Bu)3; hydroquinone in tetrahydrofuran T=55°C; 10 h;
参考文献
Journal of Organic Chemistry, , vol. 71, # 6 p. 2429 - 2433
参考文献
Tetrahedron Letters, , vol. 40, # 19 p. 3791 - 3794
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 1,3-bis-(diphenylphosphino)propane in ethylene glycol dimethyl ether T=100°C; 72 h;
参考文献
Chemistry of Heterocyclic Compounds, , vol. 37, # 12 p. 1532 - 1540
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in water; benzene Reflux;
参考文献
Organic and Biomolecular Chemistry, , vol. 6, # 16 p. 3005 - 3013
反应条件
1: lithium tert-butylate / tetrahydrofuran 2: [copperl(II)(1,1,1,5,5,5-hexafluoroacetylacetonate)2] monohydrate / toluene / 1 h / 150 °C / Inert atmosphere View Scheme
参考文献
Organic Letters, , vol. 13, # 5 p. 1110 - 1113
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.17 h / 0 °C 1.2: 0 - 20 °C 2.1: water; palladium diacetate; triphenylphosphine / tetrahydrofuran / 24 h / 50 °C View Scheme
参考文献
Organic Letters, , vol. 14, # 1 p. 390 - 393
反应条件
dichloro bis(acetonitrile) palladium(II); tri-tert-butyl phosphine; beta-naphthyl methyl ether; potassium carbonate in 1,1-dimethylpropan-1-ol T=20°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 28 p. 11408 - 11411