1-甲氧基-4-((E)-苯乙烯基)-苯合成路线 (共 30 条)
反应条件
1: 96 percent / Br2 / CH2Cl2 / 16 h
2: 50 percent / KOtBu / 2-methyl-propan-2-ol / 5 h / 50 °C
View Scheme
参考文献
Pati, Hari N.; Wicks, Martha; Holt Jr., Herman L.; LeBlanc, Regan; Weisbruch, Paul; Forrest, Lori; Lee, Moses
Heterocyclic Communications, 2005 , vol. 11, # 2 p. 117 - 120
反应条件
iodine; oxygen in cyclohexane
Irradiation;
参考文献
Letcher, R. M.
Organic Magnetic Resonance, 1981 , vol. 16, # 3 p. 220 - 223
反应条件
in acetonitrile
UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4279 - 4282
反应条件
in acetonitrile
UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2004 , vol. 69, # 12 p. 4279 - 4282
反应条件
T=25°C; 0.0333333 h; UV-irradiation; Title compound not separated from byproducts;
参考文献
Roberts, Jeffrey C.; Pincock, James A.
Journal of Organic Chemistry, 2006 , vol. 71, # 4 p. 1480 - 1492
反应条件
tert.-butylhydroperoxide; [Ru2Cl(3,6-bis(1-(2-pyridylmethyl)imidazol-2-yliden-3-yl)pyridazine)(CH3CN)4](PF6)3; sodium iodide in water; acetonitrile
T=20°C; 0.166667 h;
参考文献
Liu, Xiaolong; Chen, Wanzhi
Organometallics, 2012 , vol. 31, # 18 p. 6614 - 6622
反应条件
Oxonereg; in water; acetonitrile
14 h; Reflux;
参考文献
Parida, Keshaba Nanda; Moorthy, Jarugu Narasimha
Tetrahedron, 2014 , vol. 70, # 13 p. 2280 - 2285
反应条件
sulfuric acid; bromine in acetic acid
T=118°C; 1 h;
参考文献
Krasnokutskaya; Yusubov; Filimonov; Habicher
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 7 p. 1001 - 1004
反应条件
1: sodium hydrogencarbonate; Oxonereg; / water; acetonitrile; acetone / 5 h / 0 °C
2: carbon tetrabromide; [ruthenium(2,2′-bipyridine)2Cl2] / acetonitrile / 5 h / |Irradiation
View Scheme
参考文献
Guo, Lin; Yang, Chao; Zheng, Lewei; Xia, Wujiong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 35 p. 5787 - 5792
反应条件
Oxonereg; in water; acetonitrile
14 h; Reflux;
参考文献
Parida, Keshaba Nanda; Moorthy, Jarugu Narasimha
Tetrahedron, 2014 , vol. 70, # 13 p. 2280 - 2285