in ethanol; water Ar atmosphere; addn. of Fe-complex to soln. of NaBH4 in aq. EtOH; pouring into water, extn. (benzene);
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 33, p. 362 - 366
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 33, p. 403 - 406
in water byproducts: H2; slow addn. of H2O to a mixture of NaBH4 and ((CH3)3NH)Cl in N(CH3)3 at -10°C while stirring (3h), addn. of H2O and petroleum ether, evapn. of petroleum ether phase;;
参考文献
Gmelin Handbook: B: B-Verb.14, 3.8, page 77 - 81
Full Text Show Details
U. S. Borax & Chemical Corp.
Patent: GB952811 , 1964 ;
C. A., 1964 , vol. 61, p. 2970
