反应条件
air in diethylene glycol dimethyl ether byproducts: NaBr, H2, B; in air; simultaneous addn. of educts to reaction vessel (room temp., stirring), then heating to 65-70°C (pptn.); collection (filtration), washing (H2O, Me2CO), drying; product mixt. not sepd., detd. by powder X-ray diffraction and Moessbauer spectroscopy;
参考文献
Glavee, George N.; Klabunde, Kenneth J.; Sorensen, Christopher M.; Hadjipanayis, George C.
Inorganic Chemistry, 1995 , vol. 34, p. 28 - 35