N-Boc-DL-缬氨醇合成路线 （共 11 条）
反应条件
1: in tetrahydrofuran; water 0.166667 h; 2: With sodium tetrahydroborate in water 12 h;
参考文献
WO2014/5129 A1, ;
Page/Page column 150 ;
反应条件
lithium aluminium tetrahydride in diethyl ether Heating;
参考文献
Tetrahedron Letters, , vol. 29, # 11 p. 1265 - 1268
反应条件
1: 87 percent / DDC / DMAP / CH2Cl2 2: NBS / CCl4 / Ambient temperature; Irradiation 3: 54 percent / diethyl ether / 0.08 h / 0 °C 4: 81 percent / LiAlH4 / diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 11 p. 1265 - 1268
反应条件
1: NBS / CCl4 / Ambient temperature; Irradiation 2: 54 percent / diethyl ether / 0.08 h / 0 °C 3: 81 percent / LiAlH4 / diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 11 p. 1265 - 1268
反应条件
1: 54 percent / diethyl ether / 0.08 h / 0 °C 2: 81 percent / LiAlH4 / diethyl ether / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 29, # 11 p. 1265 - 1268
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 4 p. 563 - 568
反应条件
1.1: sodium hydroxide / 1,4-dioxane 2.1: tetrahydrofuran; water / 0.17 h 2.2: 12 h View Scheme
反应条件
1.1: sodium hydroxide / 1,4-dioxane 2.1: tetrahydrofuran; water / 0.17 h 2.2: 12 h View Scheme
反应条件
ruthenium trichloride; sodium periodate in water; acetonitrile
参考文献
Ermert, Philipp; Meyer, Jsabella; Stucki, Christoph; Schneebeli, Joerg; Obrecht, Jean-Pierre
Tetrahedron Letters, 1988 , vol. 29, # 11 p. 1265 - 1268
反应条件
sodium t-butanolate in tetrahydrofuran
参考文献
Birman, Vladimir B.; Jiang, Hui; Li, Ximin; Guo, Lei; Uffman, Eric W.
Journal of the American Chemical Society, 2006 , vol. 128, # 20 p. 6536 - 6537
