N,N-二乙基苯甲酰胺合成路线 (共 244 条)
反应条件
1: H2O; methanol / 4 h / Ambient temperature 2: 77 percent / 50percent aq. NaOH, benzyltriethylammonium chloride, O2 / dimethylsulfoxide / 2 h View Scheme
参考文献
Synthesis, , # 2 p. 109 - 110
反应条件
1: tert.-butylhydroperoxide; tetra-(n-butyl)ammonium iodide / acetonitrile; decane / 18 h / 80 °C / |Large scale 2: 12 h / 20 °C View Scheme
参考文献
RSC Advances, , vol. 3, # 44 p. 21306 - 21310
参考文献
Voronkov; Tsyrendorzhieva; Rakhlin
Russian Journal of Organic Chemistry, 2008 , vol. 44, # 4 p. 481 - 484
反应条件
potassium permanganate; N-benzyl-N,N,N-trimethyl-ammonium chloride in dichloromethane 3 h; Heating; Yield given. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 27, # 7 p. 1285 - 1290
反应条件
CuPF6(MeCN)2; caesium carbonate in xylene Heatingother reagents; Product distribution;
参考文献
Kalinin, Alexey V.; Bower, Justin F.; Riebel, Peter; Snieckus, Victor
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 2986 - 2987
反应条件
in tetrahydrofuran T=25°C; 14 h; Inert atmosphere;
参考文献
Journal of Combinatorial Chemistry, , vol. 12, # 2 p. 255 - 259
反应条件
water in chloroform-d1 T=20°C; 72 h; Inert atmosphereSchlenk technique;
参考文献
Organometallics, , vol. 31, # 15 p. 5494 - 5499
反应条件
1: hydrogenchloride; sodium nitrite / water / 0 - 5 °C 2: copper diacetate / acetonitrile / 5 h / 20 °C View Scheme
参考文献
Russian Chemical Bulletin, , vol. 62, # 6 p. 1366 - 1370
Izvestiya Akademii Nauk. Seriya Khimicheskaya, , # 6 p. 1366 - 1370,5
反应条件
potassium hydroxide; aluminum oxide in 1,4-dioxane T=60°C; 8 h; different solvents and catalysts, 2 - 6 h,; Product distribution;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 3 p. 838 - 843
反应条件
T=220 - 230°C; P=0.5 Torr; Yield given. Yields of byproduct given;
参考文献
Zeitschrift fuer Chemie (Stuttgart, Germany), , vol. 25, # 11 p. 398 - 399