N,N-二乙基苯甲酰胺合成路线 （共 244 条）
反应条件
oxygen; nitrogen(IV) oxide; ozone in 1,2-dichloro-ethane T=0°C; 7 h; Product distribution;
参考文献
Suzuki, Hitomi; Tomaru, Jun-ichiro; Murashima, Takashi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 17 p. 2413 - 2416
反应条件
1: N,N-diethyl benzamide With N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran T=-78°C; 1 h; 2: methyl iodide in tetrahydrofuran T=-78 - 20°C;
参考文献
Seganish, W. Michael; DeShong, Philip
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6790 - 6795
反应条件
sec.-butyllithium 1) cyclohexane, THF, -105 deg C, 1 h, 2) THF, -105 deg C, 1 h; Product distribution;
参考文献
Watanabe; Date; Kawanishi; Hori; Furukawa
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 10 p. 2637 - 2643
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Eaton, Philip E.; Martin, Ronald M.
Journal of Organic Chemistry, 1988 , vol. 53, # 12 p. 2728 - 2732
反应条件
Yield given. Multistep reaction;
参考文献
Eaton, Philip E.; Lee, Chih-Hung; Xiong, Yusheng
Journal of the American Chemical Society, 1989 , vol. 111, # 20 p. 8016 - 8018
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium 1) THF, cyclohexane, -78 deg C, 1 h, 2) to room temperature, 12 h; Yield given. Multistep reaction;
参考文献
De Silva; Reed; Billedeau; Wang; Norris; Snieckus
Tetrahedron, 1992 , vol. 48, # 23 p. 4863 - 4878
反应条件
1.1: sec-BuLi; TMEDA / tetrahydrofuran; cyclohexane / 0.5 h / -78 °C 1.2: 77 percent / tetrahydrofuran; cyclohexane / -78 - 20 °C 2.1: 67 percent / LDA / tetrahydrofuran / -78 - 20 °C 3.1: 67 percent / NaBH4; NaOH / methanol; H2O / 13 h / Heating View Scheme
参考文献
Mukherjee, Chandrani; De, Asish
Synlett, 2002 , # 2 p. 325 - 327
反应条件
2,2,6,6-tetramethylpiperidinyl-lithium; bromine; mercury dichloride in tetrahydrofuran T=0°C; 0.333333 h; other LiTMP/HgCl2 molar ratio, var. orthoactivated aromatic compounds; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 53, # 12 p. 2728 - 2732
反应条件
N,N,N',N,-tetramethylethylenediamine; 1,2-dibromo-1,1,2,2-tetrafluoroethane; sec.-butyllithium 1) THF, cyclohexane, -78 deg C, 1 h, 2) to room temperature, 12 h; Yield given. Multistep reaction;
参考文献
De Silva; Reed; Billedeau; Wang; Norris; Snieckus
Tetrahedron, 1992 , vol. 48, # 23 p. 4863 - 4878
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium; allyl bromide Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Casas, Ramon; Cave, Christian; D'Angelo, Jean
Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1039 - 1042
