N,N-二乙基苯甲酰胺合成路线 （共 244 条）
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in tetrahydrofuran
T=-78°C;
参考文献
Mills, R. J.; Horvath, R. F.; Sibi, M. P.; Snieckus V.
Tetrahedron Letters, 1985 , vol. 26, # 9 p. 1145 - 1148
反应条件
samarium; samarium diiodide in tetrahydrofuran
T=67°C; 4 h; Yield given. Yields of byproduct given;
参考文献
Ogawa, Akiya; Takami, Noriaki; Sekiguchi, Masahito; Ryu, Ilhyong; Kambe, Nobuaki; Sonoda, Noboru
Journal of the American Chemical Society, 1992 , vol. 114, # 22 p. 8729 - 8730
反应条件
triethylsilyllithium in hexane
3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60
反应条件
in hexane
3 h; Ambient temperature; Yields of byproduct given;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 1 p. 51 - 60
反应条件
water
1) hexane, 20 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bravo-Zhivotovskii, D. A.; Pigarev, S. D.; Kalikhman, I. D.; Vyazankina, O. A.; Vyazankin, N. S.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1838 - 1843,1654 - 1658
反应条件
Yield given. Multistep reaction;
参考文献
Iwao, M.; Mahalanabis, K. K.; Watanabe, M.; Silva, S. O. De; Snieckus, V.
Tetrahedron, 1983 , vol. 39, # 12 p. 1955 - 1962
反应条件
silver hexafluoroantimonate; [{(η5-C5Me5)RhCl}2(μ-Cl)2]; 2,2,2-trimethylacetic acid in chlorobenzene
T=45°C; 18 h; Inert atmosphereSchlenk technique;
参考文献
Wang, Honggen; Schroeder, Nils; Glorius, Frank
Angewandte Chemie - International Edition, 2013 , vol. 52, # 20 p. 5386 - 5389
Angew. Chem., 2013 , vol. 125, # 20 p. 5495 - 5499,5
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium; magnesium bromide in tetrahydrofuran
Other benzamides;
参考文献
Sibi; Miah; Snieckus
Journal of Organic Chemistry, 1984 , vol. 49, # 5 p. 737 - 742
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium; allyl bromide
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Casas, Ramon; Cave, Christian; D'Angelo, Jean
Tetrahedron Letters, 1995 , vol. 36, # 7 p. 1039 - 1042
反应条件
boron trifluoride diethyl etherate; methyllithium; lithium bromide in diethyl ether
T=-78°C; 1 h;
参考文献
Uno, Hidemitsu; Okada, Shin-ichiro; Ono, Tetsushi; Shiraishi, Yasukazu; Suzuki, Hitomi
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1504 - 1513
