1-甲基-4-硝基-1H-咪唑-2-羧酸甲酯合成路线 （共 6 条）
反应条件
1: T=40°C; 0.166667 h; 2: With sodium hydride 2 h;
参考文献
UNIVERSITY OF SASKATCHEWAN
Patent: WO2007/45096 A1, 2007 ;
Location in patent: Page/Page column 45; 86 ;
参考文献
Jaramillo, David; Liu, Qi; Aldrich-Wright, Janice; Tor, Yitzhak
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 8151 - 8153
反应条件
1: 65 percent / HNO3; H2SO4; acetic anydride / 24 h / 0 - 20 °C 2: 70 percent / methanol / 3 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 23 p. 8151 - 8153
反应条件
1: 91 percent / hydrogen / Pd/C / methanol / 31 h 2: 87 percent / potassium tert-butoxide; H2O / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Jaramillo, David; Liu, Qi; Aldrich-Wright, Janice; Tor, Yitzhak
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 8151 - 8153
反应条件
hydrogen; palladium over charcoal in methanol; ethyl acetate P=3620.13 Torr; 14 h; Product distribution / selectivity;
参考文献
UNIVERSITY OF SASKATCHEWAN
Patent: WO2007/45096 A1, 2007 ;
Location in patent: Page/Page column 87 ;
反应条件
hydrogen; palladium on activated charcoal in methanol
31 h;
参考文献
Jaramillo, David; Liu, Qi; Aldrich-Wright, Janice; Tor, Yitzhak
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 8151 - 8153
