2-乙基-4,5-二氢噻唑合成路线 (共 11 条)
反应条件
tetraphosphorus decasulfide
参考文献
Zhou, Aihua; Pittman Jr., Charles U.
Synthesis, 2006 , # 1 art. no. M01705SS, p. 37 - 48
反应条件
ammonium acetate; sodium ethanolate in ethanol 12 h; Heating;
参考文献
Fuganti, Claudio; Gatti, Francesco G.; Serra, Stefano
Tetrahedron, 2007 , vol. 63, # 22 p. 4762 - 4767
反应条件
in ethanol 5 h; Heating;
参考文献
Robbe; Fernandez; Chapat; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 1 p. 16 - 24
反应条件
phosphate buffer in water T=25°C; 0.5 h;
参考文献
Huang, Tzou-Chi; Huang, Lee-Zen; Ho, Chi-Tang
Journal of Agricultural and Food Chemistry, 1998 , vol. 46, # 1 p. 224 - 227
参考文献
Gabriel; v. Hirsch
Chemische Berichte, 1896 , vol. 29, p. 2610
反应条件
Erwaermen des Reaktionsgemisches mit P2S5;
参考文献
Bach; Zahn
Journal fuer Praktische Chemie (Leipzig), 1959 , vol. <4> 8, p. 68,70
反应条件
(i) Cl2, (ii) H2S, (iii) aq. NaOH; Multistep reaction;
参考文献
Beger,J. et al.
Journal fuer Praktische Chemie (Leipzig), 1969 , vol. 311, p. 408 - 419
反应条件
in methanol 40 h; Heating;
参考文献
Robbe; Fernandez; Chapat; et al.
European Journal of Medicinal Chemistry, 1985 , vol. 20, # 1 p. 16 - 24
反应条件
1: With tert.-butylhydroperoxide; selenium(IV) oxide in dichloromethane T=20°C; 3 h; 2: With triphenylphosphine in dichloromethane T=0°C; 12 h;
参考文献
Fuganti, Claudio; Gatti, Francesco G.; Serra, Stefano
Tetrahedron, 2007 , vol. 63, # 22 p. 4762 - 4767
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Thiel et al.
Justus Liebigs Annalen der Chemie, 1959 , vol. 622, p. 107,116