3,4-二(苄氧基)苄醇合成路线 （共 17 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Reimann,E.
Justus Liebigs Annalen der Chemie, 1971 , vol. 750, p. 109 - 127
反应条件
bis(1H-benzimidazolinium) dichromate in acetone 0.0333333 h; Heating;
参考文献
Meng, Qing-Hua; Feng, Jun-Cai; Bian, Ning-Sheng; Liu, Bin; Li, Chang-Chuan
Synthetic Communications, 1998 , vol. 28, # 6 p. 1097 - 1102
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 20 °C 2: 90 percent / morpholine; AcOH / Heating 3: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating 4: 91 percent / H2 / Pd/C / ethanol View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
反应条件
1: SOCl2 / dioxane / 20 °C 2: acetonitrile / 20 °C View Scheme
参考文献
Baxter,I. et al.
Journal of the Chemical Society, 1965 , p. 3645 - 3660
反应条件
(i) SOCl2, Et2O, (ii) /BRN= 3587243/, NaI, MeCOEt; Multistep reaction;
参考文献
Carlsson,A. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 270 - 276
反应条件
phosphorus tribromide in dichloromethane T=0 - 20°C; 1.5 h;
参考文献
Brun, Kathrin A.; Linden, Anthony; Heimgartner, Heinz
Helvetica Chimica Acta, 2002 , vol. 85, # 10 p. 3422 - 3443
反应条件
1: SOCl2 3: aq. KOH / ethanol View Scheme
参考文献
Carlsson,A. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 270 - 276
反应条件
1: (i) SOCl2, Et2O, (ii) /BRN= 3587243/, NaI, MeCOEt 2: aq. KOH / methanol; dioxane 3: (i) SOCl2, benzene, (ii) aq. NH3 4: H2 / Pd-C / ethanol View Scheme
参考文献
Helvetica Chimica Acta, , vol. 45, p. 270 - 276
反应条件
sodium tetrahydroborate in methanol
T=20°C; 1 h;
参考文献
Venkateswarlu, Somepalli; Satyanarayana, Boyina; Sureshbabu, Chillara V.; Subbaraju, Gottumukkala V.
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 11 p. 2463 - 2466
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C;
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
