3,4-二(苄氧基)苄醇合成路线 （共 17 条）
反应条件
lithium aluminium tetrahydride in diethyl ether
3 h;
参考文献
PROTEOTECH INC; ESPOSITO, Luke; HANSON, Kelsey; YADON, Marisa, C.; LAKE, Thomas; KUMAR, Anil; SNOW, Alan, D.; CUMMINGS, Joel
Patent: WO2013/62762 A1, 2013 ;
Location in patent: Page/Page column 35 ;
反应条件
1: H2SO4 / Heating
2: 86 percent / K2CO3 / dimethylformamide / 8 h / 75 °C
3: 94 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
反应条件
1: 86 percent / K2CO3 / dimethylformamide / 8 h / 75 °C
2: 94 percent / LiAlH4 / tetrahydrofuran / 0 - 20 °C
View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
反应条件
1: 89 percent / potassium carbonate / acetone / 4 h / Heating
2: 99 percent / sodium borohydride / methanol / 1 h / 20 °C
View Scheme
参考文献
Venkateswarlu, Somepalli; Satyanarayana, Boyina; Sureshbabu, Chillara V.; Subbaraju, Gottumukkala V.
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 11 p. 2463 - 2466
反应条件
1: K2CO3 / methanol / Heating
2: NaBH4 / methanol / 20 °C
View Scheme
参考文献
Lisowski, Vincent; Enguehard, Cecile; Lancelot, Jean-Charles; Caignard, Daniel-Henri; Lambel, Stephanie; Leonce, Stephane; Pierre, Alain; Atassi, Ghanem; Renard, Pierre; Rault, Sylvain
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 16 p. 2205 - 2208
反应条件
1: NaI, K2CO3 / ethanol
2: NaBH4 / propan-2-ol
View Scheme
参考文献
Yang, Li-Ming; Lin, Shwu-Jiuan; Yang, Tsang-Hsiung; Lee, Kuo-Hsiung
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 8 p. 941 - 944
反应条件
1: pyridinium chlorochromate / CH2Cl2 / 20 °C
2: 90 percent / morpholine; AcOH / Heating
3: 95 percent / p-toluenesulfonic acid monohydrate / 24 h / Heating
View Scheme
参考文献
Percec, Virgil; Peterca, Mihai; Sienkowska, Monika J.; Ilies, Marc A.; Aqad, Emad; Smidrkal, Jan; Heiney, Paul A.
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3324 - 3334
