2-(3,4-双(苄氧基)苯基)乙酸合成路线 （共 11 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=70°C; 24 h;
参考文献
He; Tadic; Brzostowska; Brossi; Bell; Creveling
Helvetica Chimica Acta, 1991 , vol. 74, # 7 p. 1399 - 1411
反应条件
potassium hydroxide; water in ethylene glycol 18 h; Heating;
参考文献
Battersby, Alan R.; Jones, Raymond C. F.; Kazlauskas, Rymantas; Thornber, Craig W.; Ruchirawat, Somsak; Staunton, James
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2016 - 2029
反应条件
potassium hydroxide in methanol; water
参考文献
Takeda Chemical Industries, Ltd.
Patent: US5047430 A1, 1991 ;
反应条件
hydrogenchloride; water in tetrahydrofuran Reflux;
参考文献
Zhang, Zhao-Li; Chen, Jinglei; Xu, Qiongming; Rao, Cui; Qiao, Chunhua
Synthetic Communications, 2012 , vol. 42, # 6 p. 794 - 798
反应条件
1: NaBH4 2: SOCl2 4: aq. KOH / ethanol View Scheme
参考文献
Zhang, Zhao-Li; Chen, Jinglei; Xu, Qiongming; Rao, Cui; Qiao, Chunhua
Synthetic Communications, 2012 , vol. 42, # 6 p. 794 - 798
反应条件
1: dimethylsulfoxide / (14)C labelling 2: KOH / ethane-1,2-diol; H2O / Heating; (14)C labelling View Scheme
参考文献
Baxter,I. et al.
Journal of the Chemical Society, 1965 , p. 3645 - 3660
反应条件
1: SOCl2 3: aq. KOH / ethanol View Scheme
参考文献
Carlsson,A. et al.
Helvetica Chimica Acta, 1962 , vol. 45, p. 270 - 276
反应条件
1: potassium carbonate / acetone / 20 h / Reflux 2: potassium hydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 3: hydrogenchloride; water / tetrahydrofuran / Reflux View Scheme
参考文献
Zhang, Zhao-Li; Chen, Jinglei; Xu, Qiongming; Rao, Cui; Qiao, Chunhua
Synthetic Communications, 2012 , vol. 42, # 6 p. 794 - 798
反应条件
1: potassium carbonate / acetone / 20 h / Reflux 2: potassium hydride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere 3: hydrogenchloride; water / tetrahydrofuran / Reflux View Scheme
参考文献
Zhang, Zhao-Li; Chen, Jinglei; Xu, Qiongming; Rao, Cui; Qiao, Chunhua
Synthetic Communications, 2012 , vol. 42, # 6 p. 794 - 798
反应条件
1: sodium tetrahydroborate; methanesulfonic acid / dimethyl sulfoxide / 20 °C 2: 10 palladium on activated charcoal; hydrogen / tetrahydrofuran / 3 h View Scheme
参考文献
Zhang, Zhao-Li; Chen, Jinglei; Xu, Qiongming; Rao, Cui; Qiao, Chunhua
Synthetic Communications, 2012 , vol. 42, # 6 p. 794 - 798
