(S)-4-异丙基-2-恶唑烷酮合成路线 (共 117 条)
反应条件
triethylamine; phosphorochloridic acid diphenyl ester in dichloromethane T=-40 - 25°C;
参考文献
Paz, Jairo; Perez-Balado, Carlos; Iglesias, Beatriz; Munoz, Luis
Journal of Organic Chemistry, 2010 , vol. 75, # 9 p. 3037 - 3046
反应条件
potassium carbonate T=125 - 126°C; 6 h;
参考文献
Evans; Mathre; Scott
Journal of Organic Chemistry, 1985 , vol. 50, # 11 p. 1830 - 1835
反应条件
lithium hydroxide; dihydrogen peroxide in tetrahydrofuran; water T=20°C; 12 h;
参考文献
Tetrahedron Asymmetry, , vol. 17, # 24 p. 3386 - 3399
反应条件
sodium in methanol; ethyl acetate; carbonic acid diethyl ester
参考文献
Immunex Corporation
Patent: US5594106 A1, 1997 ;
US 5594106 A
反应条件
oxygen; copper-(N-heterocyclic carbene) complex in 1,4-dioxane T=100°C; P=37503.8 Torr; 3 h;
参考文献
Zheng, Shuzhan; Li, Fuwei; Liu, Jianming; Xia, Chungu
Tetrahedron Letters, 2007 , vol. 48, # 33 p. 5883 - 5886
反应条件
1: With iodine in tetrachloromethane T=20°C; 1 h; 2: With lithium hydroxide; dihydrogen peroxide in tetrahydrofuran T=0°C; 1 h; Further stages.;
参考文献
Journal of the American Chemical Society, , vol. 123, # 23 p. 5602 - 5603
反应条件
(+/-)-2-Ethyloxirane; trifluoroacetic acid in dichloromethane T=0°C;
参考文献
Calo, Vinzenzo; Nacci, Angelo; Volpe, Angela
Gazzetta Chimica Italiana, 1997 , vol. 127, # 5 p. 283 - 286
反应条件
sodium tetrahydroborate in tetrahydrofuran T=20°C; 18 h;
参考文献
Palomo, Claudio; Oiarbide, Mikel; Dias, Flavia; Lopez, Rosa; Linden, Anthony
Angewandte Chemie - International Edition, 2004 , vol. 43, # 25 p. 3307 - 3310
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1.) -78 deg C, 0.5 h, 2.) 25 deg C, 2 h;
参考文献
Journal of the American Chemical Society, , vol. 112, # 13 p. 5290 - 5313
参考文献
Palomo, Claudio; Oiarbide, Mikel; Dias, Flavia; Lopez, Rosa; Linden, Anthony
Angewandte Chemie - International Edition, 2004 , vol. 43, # 25 p. 3307 - 3310