(S)-4-异丙基-2-恶唑烷酮合成路线 （共 117 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran; water T=20 - 25°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 23 p. 5602 - 5603
反应条件
sodium tetrahydroborate in tetrahydrofuran; water T=20 - 25°C; 2 h;
参考文献
Journal of the American Chemical Society, , vol. 123, # 23 p. 5602 - 5603
反应条件
1: With hydrogen; acetic acid; 20 palladium hydroxide on carbon T=50°C; P=75007.5 Torr; 22 h; 2: With hydrogenchloride in methanol; water Product distribution / selectivity;
参考文献
WO2005/49570 A1, ;
Page/Page column 15 ;
反应条件
1: With hydrogen; acetic acid; 5 rhodium on carbon T=40 - 75°C; P=112511 Torr; 42 h; 2: With hydrogenchloride in methanol; water Product distribution / selectivity;
参考文献
WO2005/49570 A1, ;
Page/Page column 17; 18 ;
反应条件
1: With hydrogen; acetic acid; 20 palladium hydroxide on carbon T=25 - 65°C; P=75007.5 Torr; 27 h; 2: With hydrogenchloride in methanol; water Product distribution / selectivity;
参考文献
WO2005/49570 A1, ;
Page/Page column 16 ;
反应条件
potassium hydroxide in water; toluene
反应条件
1: (S)-N-[3-(4-methylphenyl)-2-(E)-butenoyl]-4-isopropyl-1,3-oxazolidine-2-thione With boron trifluoride diethyl etherate in dichloromethane 7 h; cooling; 2: methanol With Sm(OTf)3 T=20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 25 p. 3307 - 3310
反应条件
1: With hydrogen; acetic acid T=50°C; P=75007.5 Torr; 21 h; 2: With hydrogenchloride in methanol; water Product distribution / selectivity;
参考文献
STUDIENGESELLSCHAFT KOHLE MBH
Patent: WO2005/49570 A1, 2005 ;
Location in patent: Page/Page column 12; 13 ;
反应条件
sodium tetrahydroborate; lithium iodide in tetrahydrofuran 8 h; Heating;
参考文献
Sudharshan, Manjula; Hultin, Philip G.
Synlett, 1997 , vol. 1997, # 2 p. 171 - 172
反应条件
1: BH3*SMe2, BF3*OEt2 2: K2CO3 View Scheme
参考文献
Heterocycles, , vol. 47, # 2 p. 765 - 780
