(S)-4-异丙基-2-恶唑烷酮合成路线 （共 117 条）
反应条件
zinc(II) chloride in acetonitrile T=20°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 14 p. 4792 - 4796
反应条件
lithium hydroxide; dihydrogen peroxide 1.) THF, water, 20 deg C, 24 h, 2.) THF, MeOH, water, 23 deg C, 24 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 112, # 10 p. 4070 - 4072
反应条件
lithium borohydride in water T=0°C; 0.666667 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 74, # 1-4 p. 401 - 402
反应条件
lithium borohydride in water T=0°C; 0.666667 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 74, # 1-4 p. 401 - 402
反应条件
lithium borohydride in water T=0°C; 0.666667 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 74, # 1-4 p. 401 - 402
反应条件
potassium carbonate in toluene 3 h; Heating; Yield given;
参考文献
Synthetic Communications, , vol. 25, # 4 p. 561 - 568
反应条件
1: 1.) dibutylboron trifluoromethanesulfonate, diisopropylethylamine, 2.) Et2AlCl / 1.) CH2Cl2, 0 deg C, 45 min, 2.) hexane, -78 deg C, 1 h 2: TsOH*H2O / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 19 p. 2411 - 2419
反应条件
1: 1.) LDA / 1.) THF, -78 deg C, 0.5 h, 2.) -20 deg C, 2 h 2: 75 percent / lithium benzyloxide / tetrahydrofuran / 1.5 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 50, # 11 p. 1830 - 1835
反应条件
1: With dihydrogen peroxide; lithium hydroxide hydrate in tetrahydrofuran; water T=-40 - 0°C; 0.583333 h; 2: With hydrogenchloride in water
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 43 p. 10856 - 10860
Angew. Chem., vol. 124, # 43 p. 11014 - 11018,5
反应条件
1: With dihydrogen peroxide; lithium hydroxide hydrate in tetrahydrofuran; water T=-40 - 0°C; 0.583333 h; 2: With hydrogenchloride in water
参考文献
Angewandte Chemie - International Edition, , vol. 51, # 43 p. 10856 - 10860
Angew. Chem., vol. 124, # 43 p. 11014 - 11018,5
