(S)-4-异丁基-2-噁唑烷酮合成路线 (共 5 条)
反应条件
caesium carbonate in dimethylsulfoxide-d6 T=25 - 150°C; P=2280.15 Torr; 24 h; Schlenk techniqueAutoclave;
参考文献
Foo, Siong Wan; Takada, Yuki; Yamazaki, Yusuke; Saito, Susumu
Tetrahedron Letters, 2013 , vol. 54, # 35 p. 4717 - 4720
反应条件
1: (1S)-1-(hydroxymethyl)-3-methylbutylamine in acetonitrile T=20°C; Electrolysis; 2: carbon dioxide 1 h; 3: p-toluenesulfonyl chloride T=20°C;
参考文献
Feroci, Marta; Gennaro, Armando; Inesi, Achille; Orsini, Monica; Palombi, Laura
Tetrahedron Letters, 2002 , vol. 43, # 33 p. 5863 - 5865
反应条件
triethylamine in dichloromethane T=4 - 20°C; Inert atmosphere;
参考文献
Begis, Guillaume; Cladingboel, David E.; Jerome, Laure; Motherwell, William B.; Sheppard, Tom D.
European Journal of Organic Chemistry, 2009 , # 10 p. 1532 - 1548
反应条件
1: BH3*SMe2, BF3*OEt2 2: K2CO3 View Scheme
参考文献
Yamamoto, Yoshinori; Onuki, Setsuko; Yumoto, Masatoshi; Asao, Naoki
Heterocycles, 1998 , vol. 47, # 2 p. 765 - 780
参考文献
Yamamoto, Yoshinori; Onuki, Setsuko; Yumoto, Masatoshi; Asao, Naoki
Heterocycles, 1998 , vol. 47, # 2 p. 765 - 780