1,4,8-三(叔丁氧碳酰)-1,4,8,11-四氮杂环十四烷合成路线 （共 6 条）
反应条件
triethylamine in dichloromethane T=20°C;
参考文献
Fabbrizzi, Luigi; Foti, Francesco; Licchelli, Maurizio; Maccarini, Paola M; Sacchi, Donatella; Zema, Michele
Chemistry (Weinheim an der Bergstrasse, Germany), 2002 , vol. 8, # 21 p. 4965 - 4972
参考文献
Boitrel, Bernard; Andrioletti, Bruno; Lachkar, Mohammed; Guilard, Roger
Tetrahedron Letters, 1995 , vol. 36, # 28 p. 4995 - 4998
反应条件
in dichloromethane 4 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Dessolin, Jean; Galea, Pascale; Vlieghe, Patrick; Chermann, Jean-Claude; Kraus, Jean-Louis
Journal of Medicinal Chemistry, 1999 , vol. 42, # 2 p. 229 - 241
反应条件
1: 53 percent / sodium carbonate / acetonitrile / 48 h / Heating 2: 90 percent / 6 M HCl / 1 h / 80 °C View Scheme
参考文献
Brandes, Stephane
Bulletin de la Societe Chimique de France, 1996 , vol. 133, # 1 p. 65 - 73
反应条件
1: 90 percent / Cs2CO3 / acetonitrile / Heating 2: 92 percent / HCl / methanol / 20 °C View Scheme
参考文献
Dong; Lindoy
Australian Journal of Chemistry, 2001 , vol. 54, # 5 p. 291 - 297
反应条件
1: 74 percent / caesium carbonate / acetonitrile / 4 h / Heating 2: 90 percent / aq. hydrochloric acid / methanol / 20 °C View Scheme
参考文献
Ramli, Martalena; Dong, Ying; Lindoy, Leonard F.; Smith, Suzanne V.; Wilson, J. Gerald
Journal of Heterocyclic Chemistry, 2005 , vol. 42, # 1 p. 77 - 83
